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河北大學化學與環(huán)境科學學院研究生導師呂運開介紹如下:
一、個人簡介
呂運開(Lv Yun-Kai),男,教授,碩士/博士研究生導師,生于1967年11月,河北省隆堯縣人。1987年6月畢業(yè)于河北大學化學系,1999年獲河北大學分析化學碩士學位,2004年獲南開大學分析化學博士學位, 2005年在河北大學化學博士后流動站工作。1987年7月至今在河北大學化學與環(huán)境科學學院任教。
聯(lián)系方式:E-mail:lvyunkai@hbu.edu.cn
二、主講課程及研究方向
[1] 主講課程:現(xiàn)代分離分析方法、分析化學進展、現(xiàn)代儀器分析、食品安全與健康。
[2] 專業(yè)與研究方向:分析化學,復雜樣品分離分析
[3] 研究領域與興趣
(1)分離分析新材料的合成及應用:手性分離材料、石墨烯復合材料、金屬有機骨架材料、功能化納米微球等;
(2)色譜-質(zhì)譜聯(lián)用技術:分析對象主要包括農(nóng)獸藥殘留、食品包裝材料、食品與中草藥屬性與真?zhèn)蔚龋?br />
(3)環(huán)境污染物的檢測、釋放規(guī)律、吸附凈化與催化降解技術;
(4)疾病標志物檢測與篩選;
(5)在線樣品預處理聯(lián)用技術。
三、主持課題
[1]河北省研究生創(chuàng)新資助項目(S201717):肝癌標志物蛋白的適配體篩選優(yōu)化及特異性分析,2017.03-2018.03
[2]河北省自然科學基金資助項目(B2016201213):金屬有機骨架復合材料的合成及其在室內(nèi)有害氣體富集檢測中應用,2016.1-2018.12
[3]開灤集團項目(合同編號:KL煤化工[2016]282號):復合材料分析檢測技術開發(fā)及其阻燃劑研究中的應用,72016.5-2017.5
[4]國家自然科學基金資助項目(21375032):基于限進介質(zhì)-分子印跡磁性微球的食品中抗生素殘留選擇性萃取凈化體系研究,2014.1-2017.12。
[5]河北省自然科學基金資助項目(B2011201081):分子印跡雜化材料制備及在線SPE-HPLC分離分析新方法研究,2011.1-2013.12。
[6]河北省應用基礎研究計劃重點基礎研究項目(10967126D):乳制品及相關食品的樣品處理新技術與有毒有害物質(zhì)關鍵檢測技術研究,2010.1-2012.12。
[7]國家自然科學基金資助項目(20675024):新型分子印跡材料制備方法的研究及其在食品安全檢測中的應用,2007.1-2009.12。
[8]河北省教育廳科學計劃項目(2006407):基于動物源食品安全分析的新型色譜分離介質(zhì)研究,2007.1-2009.12。
[9]第三十七批中國博士后科學基金(2005037629):溶膠-凝膠色譜固定相的制備及獸藥殘留分析新方法研究,2005.1-2005.12。
[10]河北大學自然科學研究計劃項目:環(huán)境中痕量有毒元素及有機污染物分離富集新技術方法研究,2005.1-2008.12。
四、獲獎情況
2007年獲天津市自然科學一等獎:金屬組學和環(huán)境化學中的分析新技術和新方法研究。
2014年獲河北省自然科學三等獎:基于多孔功能分離材料的微型化復雜樣品萃取分離技術。
2016年獲河北省科學技術進步二等獎:生物分子高靈敏度質(zhì)譜檢測新技術研究
五、代表性論文
[35] Song Aizhen, Song Jianmin, Lv Yunkai, Liang Linlin, Wang Jing*, Zhao Lei. Energy storage performance in BiMnO3-modified AgNbO3 anti-ferroelectric ceramics. Materials Letters, 2019, 237, 278-281. DOI: 10.1016/j.matlet.2018.11.105
[34] Wang Chen-Feng, Wang Zhen-Guang, Sun Xin-Yue, Chen Meng-Jiao and Lv Yun-Kai*. An ultrasensitive fluorescent aptasensor for detection of cancer marker protein based on graphene oxide-ssDNA, RSC Advances, 2018, 8, 41143-41149. DOI: 10.1039/c8ra08078j.
[33] Duan Ruijie, Wang Jing *, Jiang Shenglin, Lv Yunkai, Li Jiali, Song Aizhen, Liang Linlin. Sr2+ doping to Enhanced energy-storage properties of (Na0.5Bi0.5)0.94Ba0.06TiO3 lead-free ferroelectric ceramics. Journal of Materials Science: Materials in Electronics, 2018, 29:13952–13956, 23. DOI: 10.1007/s10854-018-9528-8
[32] 馬瑤佳, 張茜, 賈博, 呂運開*. 功能化磁性納米粒子在污水處理中的應用進展. 中國給水排水, 2018, 34(22): 31-36
[31] Zhao Ya-Ting, Yu Li-Qing, Xia Xin, Yang Xin-Yu, Hu Wei, Lv Yun-Kai*. Evaluation of adsorption and desorption properties of zeolitic imidazolate framework-7 for volatile organic compounds through thermal desorption-gas chromatography. Analytical Methods, 2018, 10(40) 4894-4901. DOI: 10.1039/C8AY01856A
[30] 張茜, 劉煒倫, 路亞楠, 呂運開*. 頂空氣相色譜-質(zhì)譜聯(lián)用技術的應用進展. 色譜, 2018, 36(10): 962-971. DOI: 10.3724/SP.J.1123.2018.0513
[29] Wang Si-Ying, Wang Chen-Feng, Lv Yun-Kai*, Shen Shi-Gang. Fabrication of fluorescent biosensing platform based on graphene oxide-dna and their application in biomolecule detection. Trends in Analytical Chemistry, 2018, 106: 53-61. DOI: https://doi.org/10.1016/j.trac.2018.07.004
[28] Zhang Qi, Wang Chen-Feng, Lv Yun-Kai*. Luminescent switch sensors for the detection of biomolecules based on metal-organic frameworks. Analyst, 2018, 143: 3761. DOI: 10.1039/C8AN00816G
[27] Liu Chang, Yu Li-Qing, Zhao Ya-Ting, Lv Yun-Kai*. Recent advances in metal-organic frameworks for adsorption of common aromatic pollutants. Microchim Acta, 2018, 185(7): 342. DOI:https://doi.org/10.1007/s00604-018-2879-2
[26] Yu Li-Qing, Wang Li-Ya, Su Fei-Hong, Hao Ping-Yu, Wang Huan, Lv Yun-Kai*. A gate-opening controlled metal-organic framework for selective solid-phase microextraction of aldehydes from exhaled breath of lung cancer patients. Microchim Acta, 2018, 185(6): 307. DOI: https://doi.org/10.1007/s00604-018-2843-1
[25] 周少丹,唐嘉琦,賈博,呂運開*. 表面接枝親水性聚合物刷磁性微球的制備及其對蜂蜜中四環(huán)素類抗生素殘留的磁分散固相萃取, 色譜, 2018, 38(2): 85-93.
[24] 馬俊琴, 于小慧, 賈翠玲, 呂運開*. 分子印跡雜化介孔硅膠材料的制備及固相萃取-高效液相色譜法測定鱈魚中氟喹諾酮類獸藥殘留. 食品安全質(zhì)量檢測學報, 2018, 9(3): 540-546
[23] 張琪,馬瑤佳,艾連峰,呂運開*. 基于輕質(zhì)萃取劑的渦旋輔助分散液液微萃取-氣相色譜法測定瓶裝水中塑化劑. 河北大學學報(自然科學版)2018, 1(38): 33-40.
[22] 董煥新, 呂二盼, 詹磊, 呂運開*. 食品中動物源性成分的多重PCR快速檢測. 食品安全質(zhì)量檢測學報, 2018, 9(17): 4595-4600.
[21] Lv Yun-Kai*, Xiong Xue, Zhao Fang-Fang, Li Meng-Zhe, Wang Mian and Li Xiao-Yang. Preparation of magnetic surface-imprinted polymer microspheres with hydrophilic external layers for selective extraction of fluoroquinolones from eggs. Australian Journal of Chemistry, 2017, 70(3): 237-244.
[20] Lv Yun-Kai*, Zhang Jing, Li Meng-Zhe, Zhou Shao-Dan, Ren Xing-Hui and Wang Jing. Fast clean-up and selective enrichment of florfenicol in milk by restricted access media molecularly imprinted magnetic microspheres based on surface-initiated photoiniferter-mediated polymerization. Analytical Methods, 2016, 8(19): 3982-3989.
[19] Lv Yun-Kai*, Zhang Jing-Qi, Guo Zhi-Yong, Zhang Wei, Sun Han-Wen. Determination of tetracyclines residues in egg, milk, and milk powder by online coupling of a precolumn packed with molecular imprinted hybrid composite materials to RP-HPLC-UV. Journal of Liquid Chromatography & Related Technologies, 2015, 38 (1): 1-7.
[18] Lv Yun-Kai*, Guo Zhi-Yong, Wang Jin-Zhi, Guo Meng-Meng, Yu Lin-Kang, Fang Hui. Preparation of a restricted access material–macroporous hybrid monolithic column – for on-line solid-phase extraction of the sulfonamides residues from honey. Analytical Methods, 2015, 7(4), 1563-1571
[17] Lv Yun-Kai*, He Yan-Dong, Xiong Xue, Wang Jin-Zhi, Wang Hai-Yan, Han Ya-Meng. Layer-by-layer fabrication of restricted access media-molecularly imprinted magnetic microspheres for magnetic dispersion microextraction of bisphenol A from milk samples. New Journal of Chemistry, 2015, 39(3), 1792-1799
[16] Lv Yun-Kai*, Zhang Wei, Guo Meng-Meng, Zhao Fang-Fang, Du Xiao-Xue. Centrifugal microextraction tube - cloud point extraction coupled with gas chromatography for simultaneous determination of six phthalate esters in mineral water. Analytical Methods, 2015, 7(2): 560-565.
[15] Lv Yun-Kai*, Zhang Jing-Qi, He Yan-Dong, Zhang Jing, Sun Han-Wen. Adsorption-controlled preparation of molecularly imprinted hybrid composites for selective extraction of tetracyclines residues from honey and milk. New Journal of Chemistry, 2014, 38 (2): 802–808.
[14] Sun Yue-Na, Qin Xin-Ying, Lv Yun-Kai*, Li Shan-Ze, Wei Chen. Simultaneous Determination of Five Phytohormones in Mungbean Sprouts of China by Micellar Electrokinetic Chromatography. Journal of Chromatographic Science, 2014, 52 (7), 725-729.
[13] Lv Yun-Kai*, Li Pan, Jiao Miao-Lun, Liu Bao-Sheng, Yang Chao. Fluorescence quenching study of moxifloxacin interaction with calf thymus DNA. Turkish Journal of Chemistry, 2014, 38(2): 202-209.
[12] Lv Yun-Kai*, Yang Lei, Liu Xiao-Hui, Guo Zhi-Yong, Sun Han-Wen. Preparation and evaluation of a novel molecularly imprinted hybrid composite monolithic column for online solid-phase extraction coupled with HPLC to detect trace fluoroquinolone residues in milk. Analytical Methods, 2013, 5(7): 1848–1855.
[11] Lv Yun-Kai*, Liu Xiao-Hui, Yan Shuai-Lei, Zhang Yan, Sun Han-Wen, Synthesis and characterization of the molecularly imprinted mesoporous silica based on the self-assembly technique for selective recognition of lomefloxacin in aqueous solution. Journal of Porous Materials, 2013, 20(5): 1345-1352.
[10] Lv Yun-Kai*, Zhao Chen-Xi, Li Pan, He Yan-Dong, Yang Zhong-Rui, Sun Han-Wen. Preparation of doxycycline - imprinted magnetic microspheres by inverse-emulsion suspension polymerization for magnetic dispersion extraction of tetracyclines from milk samples. Journal of Separation Science, 2013, 36(16): 2656-2663.
[9] Lv Yun-Kai*, Wang Li-Min, Yang Lei, Zhao Chen-Xi, Sun Han-Wen, Synthesis and application of molecularly imprinted poly(methacrylic acid)-silica hybrid composite material for selective solid-phase extraction and high-performance liquid chromatography determination of oxytetracycline residues in milk. Journal of Chromatography A, 2012, 1227: 48-53.
[8] Lv Yun-Kai*, Ma Yong, Zhao Xiao-Bo, Jia Cui-Ling, Sun Han-Wen, Grafting of norfloxacin imprinted polymeric membranes on silica surface for the selective solid-phase extraction of fluoroquinolones in fish samples. Talanta, 2012, 89: 270-275.
[7] Lv Yun-Kai*, Sun Yue-Na, Wang Li-Min, Jia Cui-Ling, Sun Han-Wen, A simple and high-throughput method of ultrasonic extraction-capillary electrophoresis for determination of melamine in milk. Analytical Methods, 2011, 3 (11), 2557-2561.
[6] Lu Yun-kai, Yan Xiu-Ping. An Imprinted Organic-Inorganic Hybrid Sorbent for Selective Separation of Cadmium from Aqueous Solution. Analytical Chemistry, 2004, 76(2): 453-457.
[5] Lu Yun-kai, Sun Han-Wen, Yuan Chun-Gang, and Yan Xiu-Ping. Simultaneous Determination of Trace Cadmium and Arsenic in Biological Samples by Hydride Generation-Double Channel Atomic Fluorescence Spectrometry. Analytical Chemistry, 2002, 74(7): 1525-1529.
[4] 呂運開*, 郭志勇, 王金治, 趙文革, 秦新英. 一種外表面親水性大孔有機-無機雜化整體柱的制備方法. 中國發(fā)明專利:ZL201410195140.9,2015-10-28.
[3] 呂運開*, 何艷冬, 熊雪, 秦新英, 孫漢文. 一種外表面親水的分子印跡磁性硅膠微球的制備方法. 中國發(fā)明專利:ZL201410195033.6,2015-12-02.
[2] 呂運開*, 張婧琦, 魏海英, 秦新英, 孫漢文. 一種外表面親水性雜化復合固相萃取吸附劑的制備方法. 中國發(fā)明專利:ZL201410195035.5,2015-12-30.
[1] 秦新英,呂運開*,楊磊. 一種恩諾沙星分子印跡整體柱的制備方法. 中國發(fā)明專利:ZL201410140078.3,2015-04-08.
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